Varying the time between adding a co-structure-directing agent and a silica source to an anionic surfactant template results in either well-ordered cubic or a novel tetragonal (P42/mnm) mesocage material by arrangement of micellar spheres of various sizes. The image shows the high-resolution transmission electron micrograph of the tetragonal structure and the corresponding electron diffraction pattern (inset).
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Garcia‐Bennett et al. (2005) studied this question.
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