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Novel polystyrene supported selenosulfones from 1% cross-linked polystyrene resin were prepared and applied to free radical cyclization reactions of 1,6-dienes followed by the subsequent “traceless” resin release by oxidation−elimination, providing a convenient method for the synthesis of methylenecyclopentanes. Apart from getting the methylenecyclopentanes, we found that cyclopentanylmethyl alcohols were formed by the oxidation−elimination of the resin, which has not been observed in solution-phase synthesis under the same conditions.
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Qian et al. (2003) studied this question.
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