Octahedral and rectangle-like LiMn2O4 single crystals larger than 0.1 × 0.1 × 0.1 mm3 in size were synthesized by evaporating a melt of LiCl and MnCl2 at 750 °C. The nucleation and growth of the crystals proceeds on the wall of a pure alumina crucible. Phase analysis showed that purity of phase was affected by MnCl2 partial pressure.
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Tang et al. (2001) studied this question.
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