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In order to prepare bulk C 3 N 4 , high-pressure pyrolysis of melamine (C 3 N 6 H 6 ) at different temperatures was carried out. The products were characterized by C, N, H element analysis, Fourier transform infrared spectroscopy, x-ray photoelectron spectroscopy, and x-ray diffractometry. The results of the analysis reveal that graphitic phase C 3 N 4 has been synthesized. It provides a novel route to synthesis of the theoretical superhard cubic C 3 N 4 and other C 3 N 4 phases from organic compounds by a high-pressure and high-temperature method.
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A et al. (2002) studied this question.
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