For the first time, the structural chemistry of a M2C2S4 core has been elucidated in two oxidation states: two-electron reduction of Cp*2Rh2(μ-C2S4)Cl2 (rS2C-CS2 = 1.45 Å) produces Cp*2Rh2(μ-C2S4) (rS2C-CS2 = 1.34 Å).
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Holloway et al. (1999) studied this question.
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