January 1, 1983Synthesis

An Improved Preparation of Enaminones from 1,3-Diketones and Ammonium Acetate or Amine Acetates

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Abstract

The reaction of R1COCR3:C(OH)R2 [R1 = Me, Ph; R2 = Me; R3 = H, allyl; R1R2 = (CH2)3, CH2CMe2CH2] with RN+H3 OAc- (R = H, Et), gave 70-98% 7 R1COCR3:CR2NHR.

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Cite This Study

Baraldi et al. (1983) studied this question.

synapsesocial.com/papers/6a709889b27f158178276dff https://doi.org/10.1055/s-1983-30557

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Abstract

The reaction of R1COCR3:C(OH)R2 [R1 = Me, Ph; R2 = Me; R3 = H, allyl; R1R2 = (CH2)3, CH2CMe2CH2] with RN+H3 OAc- (R = H, Et), gave 70-98% 7 R1COCR3:CR2NHR.