For the first time, hybrid materials with long-range order (lamellar and even 2D hexagonal) were obtained during hydrolysis–polycondensation of α,ω-bis(trimethoxysilyl)alkanes thanks to hydrophobic van-der-Waals type interactions using highly hydrophilic conditions, the nanostructure depending mainly on the alkylene chain lengths.
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Alauzun et al. (2005) studied this question.
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