The mass spectrometric behavior of the di‐TMSi derivatives of diamino‐,dihydroxy‐and aminohydroxynaphthalenes is described. The presence or lack of doubly‐charged ions in the mass spectra is correlated with substituent position. Comparison is made with the spectra of the disubstituted benzenes. Other fragmentations are discussed with supporting data from TMSi‐d 9 derivatized compounds.
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Smith et al. (1971) studied this question.
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