Reaction of Cp*RuH(COD) with HBF 4 ·OEt 2 at −76 °C produced [Cp*Ru(H 2 )(COD)]BF 4, which transformed to [Cp*Ru(η 6 -1,3,5-COT)]BF 4 on warming to room temperature. Reaction of Cp*RuH(NBD) with HBF 4 ·OEt 2 produced a mixture of nortricyclene and the novel bimetallic complex [(Cp*Ru) 2 (μ-H)(μ-C 5 H 5 −CH CH 2 )]BF 4 .
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Jia et al. (1998) studied this question.
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