The structure of (Fe,Ni)Zn 6.5 (Pearson symbol cF412) is closely related to that of Fe 22 Zn 78 [cF408; Koster & Schoone (1981). Acta Cryst. B37, 1905-1907]. Both structures may be considered as superstructures of γ-brass, but in the title structure the occupation of two fourfold positions that are vacant in Fe 22 Zn 78 leads to further distortions away from the parent structure
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Lidin et al. (1994) studied this question.
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