The title compound, NH(4)YbP(2)O(7), crystallizes in the KAlP(2)O(7) structure type and consists of distorted YbO(6) octa-hedra and bent P(2)O(7) (4-) diphosphate units forming together a three-dimensional network. There are channels in the structure running along the c axis, where the NH(4) (+) cations are located. They are connected via N-H⋯O hydrogen bonds to the terminal O atoms of the diphosphate anions.
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Fejfarová et al. (2008) studied this question.
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