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Application of square wave voltammetry (SWV), a pulse technique without renewal of the diffusion layer between waves, was demonstrated for quantitative analysis of the lanthanide concentrations. The reproducible measurement conditions in a molten salt were investigated in terms of the principal parameters such as a pulse height and a wave frequency for getting a proper calibration curve. It was observed that peak current of SWV increased when gadolinium concentration was less than 1 wt%. In addition, the total amount of lanthanides in the binary solutions of gadolinium (Gd) and lanthanum (La) was determined by the peak deconvolution of SWV curves.
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Paek et al. (2014) studied this question.
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