Vanadium dioxide is prepared by sintering, chemical transport, and deposition in an open system and the optimal preparation conditions are given. The products, prepared by these methods, are characterized by crystallographical and chemical analysis. The upper and lower phase boundary of vanadium dioxide are determined to VO2.002±0.002 and VO1.995±0.002, respectively.
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Oppermann et al. (1975) studied this question.
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