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Silicon‐29 NMR spectra were obtained for more than 20 aqueous alkaline silicate solutions containing methanol. A signal assigned to CH 3 OSi(OH) 3 or one of its deprotonated congeners was studied in detail for the first time for the solution conditions involved. Its appearance was monitored as a function of the solution compositions. The pseudo‐equilibrium constant for its formation is of the order of 0.65.
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Samadi‐Maybodi et al. (2001) studied this question.
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