A High‐Throughput Investigation of the Role of pH, Temperature, Concentration, and Time on the Synthesis of Hybrid Inorganic–Organic Materials

Four reaction parameters and their effects on the formation of cobalt succinate phases were studied by high-throughput methods. In addition to identifying two new phases, we show that higher reaction temperatures lead to products containing less water, more basic conditions favor increasingly condensed M-O-M networks (see phase diagram), and depending on the reaction time the products are formed under either kinetic or thermodynamic control.