The <110>‐oriented perovskite is very rare in the hybrid perovskites family. In this work, an unusual layered <110>‐oriented hybrid perovskite, which is stabilized by a special organic ligand, 2‐(aminoethyl)isothiourea, has been obtained. This ligand combines a primary amine and a formamidine on the two ends of one molecule. Introduction of the special ligand brings about contorted inorganic sheets in the hybrid perovskite structure. The optical properties of the new <110>‐oriented perovskite were studied.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)
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