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May 1, 1990Journal of The Electrochemical SocietyOpen Access

In Situ FTIR Spectroscopy of Iron Electrodes in Alkaline Solutions: I . Internal Reflection Spectroscopy

Helmut Neugebauer Andreas Moser Peter Strecha A. Neckel

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Abstract

In situ FTIR spectroscopic investigations of the electrochemical reactions of iron in alkaline electrolytes using the internal reflection (ATR) geometry are presented in this paper. During cyclic voltammetric experiments, is found to be the product of the oxidation reaction Fe(0) → Fe(II), and of the reduction reaction Fe(III) → Fe(II), whereas is formed at the oxidation reaction Fe(II) → Fe(III). Differences between the first and the second cycle are explained by the amount of present on the electrode surface.

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Cite This Study

Neugebauer et al. (1990) studied this question.

synapsesocial.com/papers/6a7bf48c073f483584dfa588 https://doi.org/10.1149/1.2086692

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