The intercalation of tetrabutylammonium (TBA) cations into graphite by cation exchange from a sodium-ethylenediamine graphite intercalation compound yields a single-phase first-stage product, C(44)TBA, with a gallery expansion of 0.47 nm. The gallery dimension requires an anisotropic "flattened" cation conformation.
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Sirisaksoontorn et al. (2011) studied this question.
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