An Fe 8 S 6 dodecahedron with twelve rectangular faces and a central Fe 8 ‐cube is present in the novel Fe 8 S 6 I ⊖ ion. The synthesis of this iron‐sulfur cluster ion, the structure of which is shown on the cover page, was accomplished by reaction of [Et 4 N][Fe 6 S 6 I 6 ] with iron, ammonium iodide, and iodine.
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Pohl et al. (1984) studied this question.
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