A convenient solvothermal synthesis of SnS nanoparticles from activated tin metal and elemental sulfur is reported. Through the use of diethyleneglycoldimethylether (diglyme) as a solvent, unprotected particles of Herzenbergite 20−40 nm in size were obtained at a reaction temperature of 160 °C. Powder X-ray diffraction (XRD), EDX analysis, and TEM studies showed that β-SnS is the only product.
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Schlecht et al. (2001) studied this question.
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