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Various methods of preparing the technically important ferrospinels are discussed; particular attention is given to the reactivity and homogeneity of the final mixture. The reactivity and intimacy of mixing of the initial components may be improved by the use of chemical methods of comminution and mixing, viz., thermal decomposition of the mixed chemicals, chemical precipitation of the components, or ignition of the components in a fine state of division. The use of controlled partial pressures of oxygen (CO 2 ‐CO mixtures) for the preparation of magnetite and manganese ferrite is discussed. The feasibility of the application of these methods on a commercial scale is outlined.
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George Economos (1955) studied this question.
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