Phosphole-containing hybrid calixpyrroles have been prepared by acid-promoted condensation reactions. σ 3 -Calix[1]phosphole[1]thiophene[2]pyrrole reacts with PtCl 2 (COD) to afford an unusual type of macrocyclic Pt(II)−monophosphine complex bearing a η 3 -cyclooctadienyl ligand, in which the phosphole and pyrrole units bind the Pt−Cl moiety through cooperative, noncovalent bonding interactions.
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Matano et al. (2006) studied this question.
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