A general approach to obtain pyrophosphonates is achieved by reacting arylphosphonic acids with AgNO(3) in CH(3)CN under solvothermal conditions; the process is coupled with the C-C bond cleavage of acetonitrile and the formation of novel complexes [Ag(n)(RPO(2)(O)O(2)PR)(m)](CN); the mechanism of the process is proposed.
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Guo et al. (2009) studied this question.
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