August 20, 2004Organic Process Research & Development

Molar-Scale Synthesis of 1,2:5,6-Di-O-isopropylidene-α-d-allofuranose: DMSO Oxidation of 1,2:5,6-Di-O-isopropylidene-α-d-glucofuranose and Subsequent Sodium Borohydride Reduction

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Abstract

Two variants of oxidation with DMSO followed by sodium borohydride reduction have been investigated to make the synthesis of 1,2:5,6-di- O -isopropylidene-α- d -allofuranose ( 4 ) suitable for large-scale manufacturing.

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Christensen et al. (2004) studied this question.

synapsesocial.com/papers/6a82a2ea979d337bd4440a0d https://doi.org/10.1021/op049903t

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Molar-Scale Synthesis of 1,2:5,6-Di-O-isopropylidene-α-d-allofuranose: DMSO Oxidation of 1,2:5,6-Di-O-isopropylidene-α-d-glucofuranose and Subsequent Sodium Borohydride Reduction

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Molar-Scale Synthesis of 1,2:5,6-Di-O-isopropylidene-α-d-allofuranose: DMSO Oxidation of 1,2:5,6-Di-O-isopropylidene-α-d-glucofuranose and Subsequent Sodium Borohydride Reduction

Abstract

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