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January 8, 2009ChemSusChemOpen Access

A Supported Copper Hydroxide as an Efficient, Ligand‐free, and Heterogeneous Precatalyst for 1,3‐Dipolar Cycloadditions of Organic Azides to Terminal Alkynes

Tatsuyori Katayama Keigo Kamata Kazuya Yamaguchi Noritaka Mizuno

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Abstract

Click together: The supported copper hydroxide Cu(OH)x/Al2O3 acts as an efficient heterogeneous precatalyst for the 1,3-dipolar cycloaddition of organic azides to terminal alkynes (click chemistry). The recovered Cu(OH)x/Al2O3 retains its high activity and can be reused.

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Katayama et al. (2009) studied this question.

synapsesocial.com/papers/6a82d14fec8d0a024c10b7c0 https://doi.org/10.1002/cssc.200800202

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Synapse has enriched 5 closely related papers on similar clinical questions. Consider them for comparative context:

1Click Chemistry: Diverse Chemical Function from a Few Good ReactionsOriginal Research · 2001 · 13,765 citations
2A Stepwise Huisgen Cycloaddition Process: Copper(I)-Catalyzed Regioselective “Ligation” of Azides and Terminal AlkynesOriginal Research · 2002 · 11,666 citations
3Peptidotriazoles on Solid Phase: [1,2,3]-Triazoles by Regiospecific Copper(I)-Catalyzed 1,3-Dipolar Cycloadditions of Terminal Alkynes to AzidesEarly-Phase Clinical Trial · 2002 · 8,670 citations
4Synthesis of Neoglycopolymers by a Combination of “Click Chemistry” and Living Radical PolymerizationOriginal Research · 2006 · 586 citations
5“Click” Chemistry in a Supramolecular Environment: Stabilization of Organogels by Copper(I)-Catalyzed Azide−Alkyne [3 + 2] CycloadditionOriginal Research · 2006 · 147 citations

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