A tetrameric Tl 4 [GaBr 4 ] 4 skeletal framework, whose Tl ⊕ ions are alternately coordinated by one or two mesitylene molecules, is present in the title compound. It is formed from Tl[GaBr 4 ] and mesitylene and is the first complex containing both mono‐ and bis(arene)thallium units to be characterized by X‐ray analysis.
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Schmidbaur et al. (1985) studied this question.
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