By application of a flow system, ESR spectra of transient free radicals are obtained during liquid‐phase polymerization initiated by ·CH 3 . The coupling constants of the radicals are discussed with respect to previous findings with {article}{empty}{document}\[ HO^ • \]{document} , {article}{empty}{document}\[ NH₂ \]{document} , and ·CH 2 OH initiation. Some differences in the reactions of acrylic acid with HO· and ·CH 3 are also reported. In total, the results strongly support the usual assumptions on reaction schemes of radical polymerization.
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Fischer et al. (1967) studied this question.
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