The crystal structure of Mn2Sb has been re-examined. Rotation and Laue patterns from small fragments and patterns using powdered samples confirmed the published tetragonal structure with a ----4.08, c -----6.56 A. Large single crystals were grown to make possible a study of reflections from 00/, h00 and hhO planes. Revised values of parameters are ZMn = 0"295 and ZSD ------0.280.
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Heaton et al. (1955) studied this question.