Regular, single-crystalline nanocubes of Prussian blue, Fe 4 [Fe(CN) 6 ] 3, with different sizes were synthesized in large quantities by a direct dissociation of the single-source precursor K 4 Fe(CN) 6 in acidic solution under ultrasonic conditions. The size and size distribution of the cubes strongly depends on the reaction temperature, the concentration of K 4 Fe(CN) 6 aqueous solution, and the ultrasonic condition. The probable mechanism of formation of Prussian blue is discussed.
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Wu et al. (2005) studied this question.
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