The vacuum-oven technique for quantitative sorption of a glycerol duointerlayer by montmorillonite at 35 degrees C is adapted to 130 degrees C to obtain a mono-inter-layer of glycerol, glycerol vapor relative pressure being controlled by temperature differential. Values obtained for montmorillonite agree closely with theoretical values based on liquid glycerol density, while vermiculite retains a mono-interlayer of somewhat less than liquid glycerol density.
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Milford et al. (1962) studied this question.
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