A bicapped, highly reduced vanadylpolymolybdophosphate Keggin complex [(C2H5)3NH]5[PMoV6MoVI6O40(VIVO)2], (TEA) 1, has been prepared hydrothermally and characterized by single-crystal X-ray diffraction, IR, UV/visible, cyclic voltammetry, elemental analysis, redox titration, and 51V and 31P NMR on its degradation products. The kinetics of decomposition of 1 in aqueous solution under both aerobic and anaerobic conditions is complex.
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Chen et al. (1996) studied this question.
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