Abstract [Ph 4 P] 2 [Be(N 3 ) 4 ] ( 1 ) and [PNP] 2 [Be(N 3 ) 4 ] ( 2 ; PNP=Ph 3 PNPPh 3 ) were synthesized by reacting Be(N 3 ) 2 with [Ph 4 P]N 3 and [PNP]N 3 . Compound 1 represents the first structurally characterized homoleptic beryllium azide. The electronic structure and bonding situation in the tetraazidoberyllate dianion [Be(N 3 ) 4 ] 2− were investigated by quantum‐chemical calculations (NPA, ELF, LOL).
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Naglav et al. (2017) studied this question.
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