The crystal structures of UVO5[space group Pbcm, a= 4.1231(1)Å, b= 12.3641 (1)Å, c= 7.2071 (1)Å, Z= 4] and Cs2(UO2)2V2O8[space group P21/a,a= 10.521(2)Å, b= 8.4369(9)Å, c= 7.308(3)Å, β=106.08(1)°, Z= 2], previously obtained by single-crystal X-ray diffraction, were refined using powder neutron diffraction and Rietveld analysis adapted to time-of-flight data. The main structural features of the two compounds were confirmed but more accurate oxygen positions are reported here.
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Dickens et al. (1992) studied this question.
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