A new method for the synthesis of 2′‐ O ,5‐dimethyluridine ( 5 ) has provided the title compound in a higher yield. Application of a one‐pot ribosylation methodology resulted in an efficient, high yield synthesis of 5‐methyluridine (ribothymine, 3b ). An X‐ray diffraction analysis of 5 disclosed the conformation of the sugar moiety of this nucleoside as anti , N (3′‐endo), g + .
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Lewis et al. (1993) studied this question.
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