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Precipitation behaviour in Ni-12 at. % Ti alloy was studied by means of thin foil transmission electron microscopy and electron diffraction technique. Hardness measurements showed two stage age-hardening at 500°C and 600°C. Thin foil observations revealed that the initial rapid increase in hardness was associated with the presence of superlattice. Slower second hardening was caused by the formation of modulated structure or periodic ordered structure. The increase in hardness by these periodic structures was found to be due to the internal strain hardening as originally suggested by Mott and Nabarro.
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Saito et al. (1969) studied this question.
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