Superduper: A practical and cleaner synthetic protocol for various glycosides was established by means of a recyclable solid superacid promoter in supercritical carbon dioxide (scCO2). Anomeric mixtures composed of α- and β-isomers were successfully separated by employing supercritical fluid chromatography (SFC) with scCO2 and methanol. L=leaving group, P=protecting group, ROH= sphingosine, sugar, etc.
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Li et al. (2006) studied this question.
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