We have demonstrated for the first time a solvent-free synthesis of Zn–Al layered double hydroxides, Zn–Al LDH(Cl), by grinding solid ZnO and AlCl3·6H2O and then by autoclaving at 150 °C for 1 day without the addition of water and alkaline solution.
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Chitrakar et al. (2007) studied this question.
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