Sure diisocyanate (1) exists! Those who believed that of the many conceivable C2N2O2 isomers only cyanogendi‐N‐oxide (1) could be synthesized were mistaken. It is possible to generate diisocyanate by means of matrix‐isolation techniques, to characterize it spectroscopically, and to compile data on its stability. equation image
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Maier et al. (1996) studied this question.
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