Alumina in flow: Information obtained from in situ synchrotron powder X-ray diffraction (PXRD) measurements was used to develop the first large-scale, rapid, one-step synthesis of γ-Al2O3. The data suggest a reaction mechanism that does not involve crystalline intermediates, and γ-Al2O3 was prepared at low temperature in a continuous-flow reactor using aluminum isopropoxide in 2-propanol/water without subsequent calcination.
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Lock et al. (2011) studied this question.
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