Implementation of a Temperature‐Gradient Reactor System for High‐Throughput Investigation of Phosphonate‐Based Inorganic–Organic Hybrid Compounds

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Five new Cd phosphonates were discovered in a systematic investigation of the influence of the reaction temperature besides composition and pH value on the synthesis of inorganic–organic hybrid compounds in the CdCl2/H5L/NaOH system, which was achieved by the title procedure. In the resulting crystallization diagram (see picture), each color corresponds to a different phase.