Experimental study demonstrates solvent-free reduction of silicon tetrachloride via ball milling at room temperature, highlighting an efficient route to battery-grade nano-silicon.
A highly efficient method to prepare Si nanoparticles for high-performance lithium ion batteries: direct reduction of SiCl 4 using Na metal by mechanical milling at room temperature without using any organic solvents.
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Liu et al. (2017) studied this question.
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