The radical-induced cyclization of 1,2-bis(phosphanyl)ethane and diallylphenylphosphane coordinated to a (pentamethylcyclopentadienyl)iron(II) template gives the first ten-membered triphosphorus macrocycle with three inequivalent phosphorus centers [Eq. (1); AIBN=azobisisobutyronitrile].
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Edwards et al. (2000) studied this question.
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