A rapid and efficient method has been developed for the synthesis of vicinal bromoazide directly from olefin using N -bromosuccinimide (NBS) and trimethylsilyl azide (TMSN 3 ) as the bromine and azide sources, respectively, without any catalyst in acetonitrile as solvent. The rate of reaction is remarkably fast in acetonitrile without catalyst to produce bromoazides in high yield.
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Saikia et al. (2012) studied this question.
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