Abstract 2,3‐Naphthalocyaninatoiron(II) (2,3‐NcFe) (1) is reacted with L = 1,4‐diisocyanobenzene (dib),tert‐butylisocyanide (t‐buNC), cyclohexylisocyanide (c‐hxNC), benzylisocyanide (bzNC), pyrazine (pyz), 4,4′‐bipyridine (bpy) and pyridine (py) to form the correspondingbis‐axially coordinated 2,3‐naphthalocyaninatoiron(II) compounds, 2,3‐NcFeL23, 4, 5, 6, 7, 8, 9.All 2,3‐NcFeL2‐complexes are characterized by IR‐, and if soluble enough by1H‐NMR‐ and UV/VIS‐spectroscopy, TG/DTA‐measurements and elemental analyses. The dc‐room temperature conductivities of the 2,3‐NcFeL2‐complexes are measured and found to be several orders of magnitude higher than the corresponding phthalocyaninato‐iron‐complexes PcFeL2.
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Deger et al. (1986) studied this question.
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