New organometallic molecular squares have been prepared using photochemistry, the synthesis of {(CO)4M(4,4‘-bipy)M‘(CO)4(4,4‘-bipy)}2 [M = M‘ = Cr; M = M‘ = Mo; M = Cr, M‘ = Mo] being reported in yields of 65−75%.
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Cruse et al. (1999) studied this question.
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