Short-lived radical intermediates of electron-transfer reactions have only been postulated so far. An example is species (2), assumed to occur in the reduction of the complex (1) by CrII. The first preparation and characterization of such radicals by pulse radiolysis has now been accomplished. {article}{amssymb}{empty}{document}( CH₃)₂ C•1pt--- OH{document} (from solvent isopropanol) served as electron-transfer agent.
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Wieghardt et al. (1978) studied this question.
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