In the radical polymerization of o‐divinylbenzene, soluble polymers were obtained. The content of pendant double bond in the polymer was found to be lower than one for one monomer unit. It was concluded that the intramolecular cyclization reaction occurred during the polymerization. The effects of polymerization temperature and monomer concentration on the cyclization reaction were investigated with the aid of an equation derived kinetically.
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Aso et al. (1963) studied this question.
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