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The calixarenes tert-butylcalix[6]arene (H6L) and tert-butylcalix[8]arene (H8L′) on treatment with [V(NBut)(OBut)3] and [V(Ntolyl-p)(OBut)3] respectively afford the novel metallocalix[6] and [8]arenes [{V(NBut)(thf)0.39(ButOH)0.61}{VO(μ-O)}2L][ButNH3] (1) and [V2(NR′)2(H2L′)] (2).
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Gibson et al. (2001) studied this question.
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