The crystal structure of Li(thf)PHCy (thf = tetrahydrofuran, Cy = cyclohexyl) shows a polymeric structure with five-coordinate phosphorus atoms and four-coordinate lithium atoms. Three different Li-P distances are observed, which range from 2.608(8) to 2.631(8) Å.
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Hey‐Hawkins et al. (1994) studied this question.
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