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Abstract 4-(N,N-Dimethylamino)pyridine (dmap) reacts with [{RhCl(nbd)}2] to give [RhCl(nbd)(dmap)] (1), which was characterized by X-ray crystallography and NMR spectroscopy. The crystal structure and dynamic behavior of the molecule in solution are compared with those of [RhCl(nbd)(PPh3)] (2).
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Takenaka et al. (2000) studied this question.
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